Organic Synthesis (OCR A-Level Chemistry A): Quizzes

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Further Practical Techniques
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What is the main advantage of filtration under reduced pressure over gravity filtration?

It is significantly faster

Why must the filter paper be wetted before adding the sample in reduced pressure filtration?

Creates better seal, prevents solid passing

What property difference does recrystallisation exploit to purify solid products?

Differences in solubility

Why should minimum solvent volume be used during recrystallisation?

To maximize yield of pure product

Which solvent property is ideal for recrystallisation?

Dissolves product readily when hot

What two effects do impurities have on the melting point of a solid?

Wider range and lower temperature

What melting range indicates a highly pure organic compound?

12°C1-2\,°C

Why must heating be slow when approaching the melting point during determination?

To obtain accurate measurements

Which piece of equipment is the thick-walled conical flask with a side arm?

Büchner flask

Why must the recrystallisation mixture be cooled before filtering?

To maximize crystal formation and yield

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